Scope of Accreditation

Laboratory Name: Testmark Laboratories Ltd. (Mississauga)

Client ID: 1003751

Parent Institution: Testmark Laboratories Ltd.

Address: 6820 Kitimat Rd., Unit 4, Mississauga, Ontario, L5N 5M3

Contact: Mr. Brad Woodward

Email: brad.woodward@testmark.ca; qaqc@testmark.ca

Phone: (905) 821-1112

Fax: (905) 821-2095

Standard: Conforms with requirements of ISO/IEC 17025:2017

Clients Served: All Interested Parties

Revised On: 12/07/2024

Valid To: 04/07/2027

CALA is committed to Canada's anti-spam legislation (CASL). Please note that the email addresses published on this website are provided solely for professional or informational purposes. Any use of these addresses for unsolicited commercial electronic messages or the harvesting of email addresses is strictly prohibited and may be subject to legal action under CASL.

001 - Acidity OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: TITRIMETRIC

Preparation Method:

Lab Method ID(s): A24.0

Method Reference Modified From Analytical Method Preparation Method
SM 2310 B Yes Yes No
Parameter
Acidity

003 - Anions

Field of Accreditation: Environmental

Matrix: Solids

Analytical Method: ION CHROMATOGRAPHY (IC)

Preparation Method: EXTRACTION

Lab Method ID(s): A5

Method Reference Modified From Analytical Method Preparation Method
EPA 1311 Yes No Yes
EPA 9056A Yes Yes No
Parameter
Fluoride
Nitrate
Nitrite (NO2)

004 - Anions

Field of Accreditation: Environmental

Matrix: Solids [Soil]

Analytical Method: ION CHROMATOGRAPHY (IC)

Preparation Method:

Lab Method ID(s): A5

Method Reference Modified From Analytical Method Preparation Method
EPA 9056A Yes Yes No
Parameter
Bromide
Chloride
Fluoride
Nitrate-N
Nitrite (NO2)
Sulphate

005 - Anions OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: ION CHROMATOGRAPHY (IC)

Preparation Method:

Lab Method ID(s): A5

Method Reference Modified From Analytical Method Preparation Method
EPA 9056A Yes Yes No
Parameter
Bromide
Chloride
Fluoride
Nitrate
Nitrite
Sulfate

006 - Biochemical Oxygen Demand (BOD) OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: DISSOLVED OXYGEN METER (DO)

Preparation Method:

Lab Method ID(s): A3

Method Reference Modified From Analytical Method Preparation Method
SM 5210 B Yes Yes No
Parameter
BOD (5 day)
CBOD (5 day)
Dissolved Oxygen (DO)

007 - Carbon OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: INFRARED SPECTROSCOPY (IR)

Preparation Method: UV-PERSULPHATE OXIDATION

Lab Method ID(s): A55

Method Reference Modified From Analytical Method Preparation Method
SM 5310 C Yes Yes No
Parameter
Inorganic Carbon
Organic Carbon

008 - Chemical Oxygen Demand (COD)

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: TITRIMETRIC

Preparation Method:

Lab Method ID(s): T04

Method Reference Modified From Analytical Method Preparation Method
SM 5220 C Yes Yes No
Parameter
COD

009 - Coliforms OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: MEMBRANE FILTRATION (DC)

Preparation Method:

Lab Method ID(s): A10

Method Reference Modified From Analytical Method Preparation Method
ON MECP E3407 Yes Yes No
Parameter
Background Counts
Escherichia coli
Total Coliforms

010 - Colour OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method:

Lab Method ID(s): A26

Method Reference Modified From Analytical Method Preparation Method
SM 2120 C Yes Yes No
Parameter
Apparent Colour
True Colour

011 - Conductivity

Field of Accreditation: Environmental

Matrix: Solids [Soil]

Analytical Method: CONDUCTIVITY METER

Preparation Method:

Lab Method ID(s): A12

Method Reference Modified From Analytical Method Preparation Method
SM 2510 B Yes Yes No
Parameter
Conductivity

013 - Cyanide

Field of Accreditation: Environmental

Matrix: Solids

Analytical Method: COLORIMETRIC

Preparation Method: DISTILLATION

Lab Method ID(s): T43

Method Reference Modified From Analytical Method Preparation Method
SM 4500 CN- E Yes Yes No
EPA 335.3 Yes Yes No
ASTM D7237-10 Yes Yes No
Parameter
Cyanide (WAD)
Free Cyanide
Total Cyanide

014 - Cyanide

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method: DISTILLATION

Lab Method ID(s): T43

Method Reference Modified From Analytical Method Preparation Method
SM 4500-CN- E Yes Yes No
EPA 335.3 Yes Yes No
Parameter
Cyanide (SAD)
Cyanide (WAD)
Free Cyanide
Total Cyanide

015 - Dissolved Metals OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: ICP/MS

Preparation Method:

Lab Method ID(s): A13

Method Reference Modified From Analytical Method Preparation Method
EPA 6020B Yes Yes No
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Bismuth
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Uranium
Vanadium
Zinc

016 - Hexavalent Chromium

Field of Accreditation: Environmental

Matrix: Solids

Analytical Method: COLORIMETRIC

Preparation Method:

Lab Method ID(s): A83

Method Reference Modified From Analytical Method Preparation Method
EPA 3060A Yes Yes No
SM 3500-CR B Yes Yes No
Parameter
Hexavalent Chromium

017 - Hexavalent Chromium OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method:

Lab Method ID(s): A83

Method Reference Modified From Analytical Method Preparation Method
SM 3500-CR B Yes Yes No
Parameter
Hexavalent Chromium

018 - Heterotrophic Plate Count (HPC) OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: SPREAD PLATE

Preparation Method:

Lab Method ID(s): A68

Method Reference Modified From Analytical Method Preparation Method
ON MECP E3408 Yes Yes No
Parameter
Heterotrophic Plate Count (HPC)

019 - Metals

Field of Accreditation: Environmental

Matrix: Solids

Analytical Method: ICP/MS

Preparation Method: EXTRACTION

Lab Method ID(s): A13, A79

Method Reference Modified From Analytical Method Preparation Method
EPA 1311 Yes No Yes
EPA 6020B Yes Yes No
Parameter
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Chromium
Cobalt
Copper
Lead
Mercury
Nickel
Selenium
Silver
Thallium
Uranium
Zinc

020 - Metals

Field of Accreditation: Environmental

Matrix: Solids [Soil]

Analytical Method: ICP/MS

Preparation Method: DIGESTION

Lab Method ID(s): A13, A52

Method Reference Modified From Analytical Method Preparation Method
BC MOE LABORATORY MANUAL, SALM Yes No Yes
EPA 6020B Yes Yes No
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lanthanum
Lead
Magnesium
Manganese
Mercury
Molybdenum
Nickel
Selenium
Silver
Strontium
Thallium
Tin
Titanium
Uranium
Vanadium
Zinc

023 - Polychlorinated Biphenyls (PCB)

Field of Accreditation: Environmental

Matrix: Oil

Analytical Method: GC/ECD

Preparation Method:

Lab Method ID(s): T19

Method Reference Modified From Analytical Method Preparation Method
EPA 8082A Yes Yes No
Parameter
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Total PCB

024 - Polychlorinated Biphenyls (PCB)

Field of Accreditation: Environmental

Matrix: Solids

Analytical Method: GC/ECD

Preparation Method: EXTRACTION

Lab Method ID(s): T19

Method Reference Modified From Analytical Method Preparation Method
EPA 8082A Yes Yes No
Parameter
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Total PCB

025 - Polychlorinated Biphenyls (PCB) OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: GC/ECD

Preparation Method: EXTRACTION

Lab Method ID(s): T19

Method Reference Modified From Analytical Method Preparation Method
EPA 8082A Yes Yes No
Parameter
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Total PCB

026 - pH

Field of Accreditation: Environmental

Matrix: Solids

Analytical Method: PH METER

Preparation Method:

Lab Method ID(s): A2.0

Method Reference Modified From Analytical Method Preparation Method
EPA 9045D Yes Yes No
O.REG. 153/04 Yes Yes No
Parameter
pH

028 - Petroleum Hydrocarbons (PHC)

Field of Accreditation: Environmental

Matrix: Solids [Soil]

Analytical Method: GC/FID

Preparation Method: EXTRACTION

Lab Method ID(s): A59

Method Reference Modified From Analytical Method Preparation Method
CCME CWS PETROLEUM HYDROCARBONS IN SOIL - TIER 1 METHOD, PUBLICATION #1310 No Yes No
Parameter
F2: C10-C16
F3: C16-C34
F4: C34-C50

029 - Petroleum Hydrocarbons (PHC)

Field of Accreditation: Environmental

Matrix: Solids [Soil]

Analytical Method: GRAVIMETRIC

Preparation Method:

Lab Method ID(s): A59

Method Reference Modified From Analytical Method Preparation Method
CCME CWS PETROLEUM HYDROCARBONS IN SOIL - TIER 1 METHOD, PUBLICATION #1310 No Yes No
Parameter
F4: Gravimetric

030 - Phenols OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method: DISTILLATION

Lab Method ID(s): T38

Method Reference Modified From Analytical Method Preparation Method
SM 5530 Yes Yes No
Parameter
Total Phenolics

033 - Reactive Silica OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method:

Lab Method ID(s): A7

Method Reference Modified From Analytical Method Preparation Method
EPA 366.0 Yes Yes No
Parameter
Reactive Silica

034 - Solids OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: GRAVIMETRIC

Preparation Method:

Lab Method ID(s): A27

Method Reference Modified From Analytical Method Preparation Method
SM 2540 C Yes Yes No
SM 2540 D Yes Yes No
SM 2540 G Yes Yes No
Parameter
Total Dissolved Solids
Total Solids (TS)
Total Solids (TS) (calculation)
Total Suspended Solids
Volatile Suspended Solids

038 - Turbidity OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: NEPHELOMETRIC

Preparation Method:

Lab Method ID(s): A21

Method Reference Modified From Analytical Method Preparation Method
SM 2130 B Yes Yes No
Parameter
Turbidity

039 - Volatile Organic Compounds (VOC)

Field of Accreditation: Environmental

Matrix: Solids

Analytical Method: GC/MS-PURGE AND TRAP

Preparation Method: EXTRACTION

Lab Method ID(s): A14

Method Reference Modified From Analytical Method Preparation Method
EPA 1311 Yes No Yes
EPA 524.3 Yes Yes No
Parameter
1,1-Dichloroethene (1,1-Dichloroethylene)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,4-Dichlorobenzene
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroethene (Vinyl chloride)
Chloroform
Dichloromethane
Dichloromethane (Methylene Chloride)
Methyl ethyl ketone
Methyl isobutyl ketone (MIBK)
Tetrachloroethylene
Trichloroethylene

040 - Volatile Organic Compounds (VOC)

Field of Accreditation: Environmental

Matrix: Solids [Soil]

Analytical Method: GC/MS-PURGE AND TRAP

Preparation Method:

Lab Method ID(s): A14

Method Reference Modified From Analytical Method Preparation Method
EPA 524.3 Yes Yes No
EPA 8260D Yes Yes No
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Acetone (2-Propanone)
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethene (Vinyl chloride)
Chloroform
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropene
Dichlorodifluoromethane (CFC-12, Freon 12)
Dichloromethane
Ethylbenzene
Ethylene Dibromide
Hexane (n-Hexane)
m,p-Xylene
Methyl ethyl ketone
Methyl isobutyl ketone (MIBK)
Methyl t-butyl ether
o-Xylene
Styrene
Tetrachloroethylene
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropene
Trichloroethylene
Trichlorofluoromethane

041 - Volatile Organic Compounds (VOC) OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: GC/MS-PURGE AND TRAP

Preparation Method:

Lab Method ID(s): A14

Method Reference Modified From Analytical Method Preparation Method
EPA 524.3 Yes Yes No
EPA 8260D Yes Yes No
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Acetone (2-Propanone)
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroform
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropene
Dichlorodifluoromethane (CFC-12, Freon 12)
Dichloromethane
Ethylbenzene
Ethylene Dibromide
Hexane (n-Hexane)
m,p-Xylene
Methyl ethyl ketone
Methyl isobutyl ketone (MIBK)
Methyl t-butyl ether
o-Xylene
Styrene
Tetrachloroethylene
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropene
Trichloroethylene
Trichlorofluoromethane
Vinyl chloride

043 - Polychlorinated Biphenyls (PCB)

Field of Accreditation: Environmental

Matrix: Solids

Analytical Method: GC/ECD

Preparation Method: EXTRACTION

Lab Method ID(s): T19

Method Reference Modified From Analytical Method Preparation Method
EPA 1311 Yes No Yes
EPA 8082A Yes Yes No
Parameter
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Total PCBs (Total Polychlorinated Biphenyls)

045 - Petroleum Hydrocarbons (PHC) OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: GC/FID

Preparation Method: EXTRACTION

Lab Method ID(s): A59

Method Reference Modified From Analytical Method Preparation Method
ON MECP E3421 Yes Yes No
Parameter
F2: C10-C16
F3: C16-C34
F4: C34-C50

046 - Petroleum Hydrocarbons (PHC) OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: GRAVIMETRIC

Preparation Method:

Lab Method ID(s): A59

Method Reference Modified From Analytical Method Preparation Method
ON MECP E3421 Yes Yes No
Parameter
F4: Gravimetric

047 - Redox Potential (ORP) OSDWA

Field of Accreditation: Environmental

Matrix: Solids [Soil]

Analytical Method: ION SELECTIVE ELECTRODE (ISE)

Preparation Method: EXTRACTION

Lab Method ID(s): T06

Method Reference Modified From Analytical Method Preparation Method
SM 2580 Yes Yes No
Parameter
Redox Potential (ORP)

048 - Redox Potential (ORP)

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: ION SELECTIVE ELECTRODE (ISE)

Preparation Method:

Lab Method ID(s): T06

Method Reference Modified From Analytical Method Preparation Method
SM 2580 Yes Yes No
Parameter
Redox Potential (ORP)

049 - Total Metals OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: ICP/MS

Preparation Method: DIGESTION

Lab Method ID(s): A13, A52

Method Reference Modified From Analytical Method Preparation Method
EPA 6020B Yes Yes No
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Bismuth
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Uranium
Vanadium
Zinc

051 - Hot Water Extractable Boron

Field of Accreditation: Environmental

Matrix: Solids [Soil]

Analytical Method: ICP/MS

Preparation Method: EXTRACTION

Lab Method ID(s): A13, A52

Method Reference Modified From Analytical Method Preparation Method
GUPTA, 1967, SOIL SCIENCE 103: 424-428 Yes Yes No
Parameter
Hot Water Extractable Boron (Boron (Hot Water Soluble))

053 - Cyanide

Field of Accreditation: Environmental

Matrix: Solids

Analytical Method: COLORIMETRIC

Preparation Method: EXTRACTION

Lab Method ID(s): T43

Method Reference Modified From Analytical Method Preparation Method
EPA 1311 No No Yes
SM 4500-CN- E Yes Yes No
Parameter
Cyanide (WAD)

054 - Conductivity OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: CONDUCTIVITY METER

Preparation Method:

Lab Method ID(s): A12

Method Reference Modified From Analytical Method Preparation Method
SM 2510 B Yes Yes No
Parameter
Conductivity (25˚C)

056 - pH OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: PH METER

Preparation Method:

Lab Method ID(s): A2.0

Method Reference Modified From Analytical Method Preparation Method
SM 4500-H+ B Yes Yes No
Parameter
pH

058 - Volatile Organic Compounds (VOC) OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: GC/MS-HEADSPACE

Preparation Method:

Lab Method ID(s): A127

Method Reference Modified From Analytical Method Preparation Method
ON MECP E3421 Yes Yes No
Parameter
1,1,1,2-Tetrachloroethane
1,1-Dichloropropene
1,2,4-Trichlorobenzene
1,2-Dibromo-3-chloropropane (DBCP)
1,3-Dichloropropane
Benzene
Bromobenzene
Bromochloromethane
Bromomethane
Chlorodibromomethane
Chloroethane (Ethyl chloride)
Chloromethane (Methyl chloride)
Dichlorodifluoromethane (CFC-12, Freon 12)
Ethylbenzene
Ethylene Dibromide
Hexane (n-Hexane)
m,p-Xylene
o-Xylene
p-Dioxane
Toluene

059 - Petroleum Hydrocarbons (PHC) OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: GC/FID-HEADSPACE

Preparation Method:

Lab Method ID(s): A127

Method Reference Modified From Analytical Method Preparation Method
ON MECP E3421 Yes Yes No
Parameter
F1: C6-C10

062 - Alkalinity OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: TITRIMETRIC

Preparation Method:

Lab Method ID(s): A1.0

Method Reference Modified From Analytical Method Preparation Method
SM 2320 B Yes Yes No
Parameter
Alkalinity (pH 4.5)

066 - Volatile Organic Compounds (VOC)

Field of Accreditation: Environmental

Matrix: Solids [Soil]

Analytical Method: GC/MS-HEADSPACE

Preparation Method:

Lab Method ID(s): A127

Method Reference Modified From Analytical Method Preparation Method
EPA 524.3 Yes Yes No
EPA 624 Yes Yes No
Parameter
1,1,1,2-Tetrachloroethane
1,1-Dichloropropene
1,2,4-Trichlorobenzene
1,2-Dibromo-3-chloropropane (DBCP)
1,3-Dichloropropane
Benzene
Bromobenzene
Bromochloromethane
Bromomethane
Chloroethane (Ethyl chloride)
Chloromethane (Methyl chloride)
Dichlorodifluoromethane (CFC-12, Freon 12)
Ethylbenzene
Ethylene Dibromide
Hexane (n-Hexane)
m,p-Xylene
o-Xylene
p-Dioxane
Toluene

067 - Petroleum Hydrocarbons (PHC)

Field of Accreditation: Environmental

Matrix: Solids [Soil]

Analytical Method: GC/FID-HEADSPACE

Preparation Method:

Lab Method ID(s): A127

Method Reference Modified From Analytical Method Preparation Method
CCME CWS PETROLEUM HYDROCARBONS IN SOIL - TIER 1 METHOD, PUBLICATION #1310 No Yes No
Parameter
F1: C6-C10

070 - Alkalinity

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method:

Lab Method ID(s): A1.1

Method Reference Modified From Analytical Method Preparation Method
EPA 310.2 Yes Yes No
Parameter
Alkalinity (pH 4.5)

071 - Ammonia

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method:

Lab Method ID(s): A42

Method Reference Modified From Analytical Method Preparation Method
EPA 350.1 Yes Yes No
Parameter
Ammonia

072 - Fecal (Thermotolerant) Coliforms

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: MEMBRANE FILTRATION (M-FC WITH ROSOLIC ACID)

Preparation Method:

Lab Method ID(s): A10

Method Reference Modified From Analytical Method Preparation Method
SM 9222 B Yes Yes No
Parameter
Fecal (Thermotolerant) Coliforms

073 - Nitrate plus Nitrite and Nitrite

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method:

Lab Method ID(s): A126

Method Reference Modified From Analytical Method Preparation Method
EPA 353.1 Yes Yes No
EPA 354.1 Yes Yes No
Parameter
Nitrate plus Nitrite
Nitrite

074 - Sulphate (Sulfate)

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: TURBIDIMETRIC

Preparation Method:

Lab Method ID(s): A5.4

Method Reference Modified From Analytical Method Preparation Method
EPA 375.4 Yes Yes No
Parameter
Sulfate

075 - Total Kjeldahl Nitrogen (TKN)

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method: DIGESTION

Lab Method ID(s): A58

Method Reference Modified From Analytical Method Preparation Method
EPA 351.2 Yes Yes No
SM 4500-NORG D Yes Yes No
Parameter
Total Kjeldahl Nitrogen

076 - Phosphate OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method: DIGESTION

Lab Method ID(s): A23

Method Reference Modified From Analytical Method Preparation Method
EPA 365.3 Yes Yes No
ESS 310.2 Yes Yes No
SM 4500 P Yes Yes No
Parameter
Dissolved Reactive Phosphorus
Phosphate
Total Dissolved Phosphorus
Total Phosphorus

077 - Relative Density

Field of Accreditation: Petroleum

Matrix: Oil

Analytical Method: HYDROMETER

Preparation Method:

Lab Method ID(s): O100.10

Method Reference Modified From Analytical Method Preparation Method
ASTM D1298-12B Yes Yes No
Parameter
Relative Density

078 - Acid Number

Field of Accreditation: Petroleum

Matrix: Oil

Analytical Method: TITRIMETRIC

Preparation Method:

Lab Method ID(s): O100.6

Method Reference Modified From Analytical Method Preparation Method
ASTM D974-14E2 Yes Yes No
Parameter
Acid Number

079 - Colour

Field of Accreditation: Petroleum

Matrix: Oil

Analytical Method: COLOUR COMPARATOR

Preparation Method:

Lab Method ID(s): O100.9

Method Reference Modified From Analytical Method Preparation Method
ASTM D1500-12 Yes Yes No
Parameter
Colour

080 - Moisture

Field of Accreditation: Petroleum

Matrix: Oil

Analytical Method: COULOMETRIC TITRATION

Preparation Method:

Lab Method ID(s): O100.02

Method Reference Modified From Analytical Method Preparation Method
ASTM D1533 No Yes No
Parameter
Water

081 - Dissolved Gases

Field of Accreditation: Petroleum

Matrix: Oil

Analytical Method: GC/FID

Preparation Method:

Lab Method ID(s): O100.1

Method Reference Modified From Analytical Method Preparation Method
ASTM D3612 Yes Yes No
Parameter
Acetylene
Carbon dioxide (CO2)
Carbon monoxide (CO)
Ethane
Ethene (Ethylene)
Hydrogen
Methane
Nitrogen
Oxygen

082 - Dielectric Breakdown

Field of Accreditation: Petroleum

Matrix: Oil [Transformer]

Analytical Method: DIELECTRIC TESTER

Preparation Method:

Lab Method ID(s): O100.4

Method Reference Modified From Analytical Method Preparation Method
ASTM D1816 Yes Yes No
Parameter
Dielectric Strength

083 - Dielectric Breakdown

Field of Accreditation: Petroleum

Matrix: Oil [Transformer]

Analytical Method: DIELECTRIC TESTER

Preparation Method:

Lab Method ID(s): O100.3

Method Reference Modified From Analytical Method Preparation Method
ASTM D877-02 Yes Yes No
Parameter
Dielectric Strength

084 - Furanic Compounds

Field of Accreditation: Petroleum

Matrix: Oil [Transformer]

Analytical Method: HPLC/UV

Preparation Method: EXTRACTION

Lab Method ID(s): O100.8

Method Reference Modified From Analytical Method Preparation Method
ASTM D5837 Yes Yes No
Parameter
2-Acetylfuran
2-Furfuryl alcohol
5-Hydroxymethoxyfurfural
5-Methylfurfural
Furfural (2-Furaldehyde, Furfuraldehyde)

085 - Inhibitors

Field of Accreditation: Petroleum

Matrix: Oil

Analytical Method: FTIR

Preparation Method:

Lab Method ID(s): O100.16

Method Reference Modified From Analytical Method Preparation Method
ASTM D2668 Yes Yes No
Parameter
2,6-Di-tert-butyl-4-methylphenol (2,6-Di-tert-butyl-p-cresol, Butylated hydroxytoluene (BHT))

086 - Metals

Field of Accreditation: Petroleum

Matrix: Oil

Analytical Method: ICP/OES

Preparation Method:

Lab Method ID(s): O100.14

Method Reference Modified From Analytical Method Preparation Method
ASTM D7151 Yes Yes No
Parameter
Aluminum
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Silicon
Silver
Sodium
Tin
Tungsten
Vanadium
Zinc

087 - Oil and Grease

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: GRAVIMETRIC

Preparation Method:

Lab Method ID(s): A54

Method Reference Modified From Analytical Method Preparation Method
EPA 1664B Yes Yes No
Parameter
Total Oil and Grease

088 - Power Factor

Field of Accreditation: Petroleum

Matrix: Oil [Transformer]

Analytical Method: POWER DISSIPATION BRIDGE

Preparation Method:

Lab Method ID(s): O100.7

Method Reference Modified From Analytical Method Preparation Method
ASTM D924 Yes Yes No
Parameter
Power Dissipation

089 - Corrosive Sulfur

Field of Accreditation: Petroleum

Matrix: Oil

Analytical Method: VISUAL EXAMINATION

Preparation Method:

Lab Method ID(s): O100.13

Method Reference Modified From Analytical Method Preparation Method
ASTM D1275 Yes Yes No
Parameter
Corrosive Sulfur

090 - Interfacial Tension

Field of Accreditation: Petroleum

Matrix: Oil

Analytical Method: TENSIOMETER

Preparation Method:

Lab Method ID(s): O100.5

Method Reference Modified From Analytical Method Preparation Method
ASTM D971 Yes Yes No
Parameter
Interfacial Tension

091 - Viscosity (40 degrees)

Field of Accreditation: Petroleum

Matrix: Oil

Analytical Method: VISCOMETER

Preparation Method:

Lab Method ID(s): O100.11

Method Reference Modified From Analytical Method Preparation Method
ASTM D445 Yes Yes No
Parameter
Kinematic Viscosity

092 - UV Absorbance OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method:

Lab Method ID(s): A125

Method Reference Modified From Analytical Method Preparation Method
SM 5910 B Yes Yes No
Parameter
UV Absorbance
UV Transmittance

093 - Microcystins OSDWA

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: ENZYME-LINKED IMMUNOSORBENT ASSAY (ELISA)

Preparation Method:

Lab Method ID(s): A88

Method Reference Modified From Analytical Method Preparation Method
ABRAXIS (ADDA)-DM ELISA INSTRUCTIONS Yes Yes No
Parameter
Microcystins

094 - Chemical Oxygen Demand (COD)

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method: DIGESTION

Lab Method ID(s): A4

Method Reference Modified From Analytical Method Preparation Method
SM 5220 Yes Yes No
Parameter
Chemical Oxygen Demand (COD)

095 - Sulphide

Field of Accreditation: Environmental

Matrix: Water

Analytical Method: COLORIMETRIC

Preparation Method:

Lab Method ID(s): A11

Method Reference Modified From Analytical Method Preparation Method
SM 4500 S2- Yes Yes No
Parameter
Sulphide (Sulfide)

† “OSDWA” indicates the appendix is used for the analysis of Ontario drinking water samples, which is subject to the rules and related regulations under the Ontario “Safe Drinking Water Act” (2002).

The list of tests and measurement capabilities for which a laboratory is accredited can change at any time due to circumstances such as scope extensions, voluntary withdrawal of tests by the laboratory and suspension. Scopes are published by the CALA via the Internet at https://directory.cala.ca/

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